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OJVRTM

Online Journal of Veterinary Research©

Volume 19(11): 721-731, 2015.


Cibracon blue coated magnetic nanoparticles for detection of diazinon in apples

 

Marziyeh Mojaver, Sohrab Imani¹, Homayon Ahmad Panahi2, Khalil Talebi3

 

1Department of Entomology, College of Agriculture, Tehran Science and Research Branch, 2Department of chemistry, Central Tehran Branch, Islamic  Azad University, Tehran, 3Faculty of Agricultural Sciences & Engineering, Department of Plant Protection, College of Agriculture and Natural Resources, University of Tehran, Karaj, Iran.

 

ABSTRACT

 

Mojaver M, Imani S, Panahi HA, Talebi K., Magnetic nanoparticles for determination of diazinon in apples, Onl J Vet Res.,  19(11): 721-731, 2015. iron modified-magnetic cibracon blue coated nanoparticles (MNP) were used for magnetic solid-phase (MSPE) sorbent extraction for determination of diazinon residue in apples. Test results were compared with high performance liquid chromatography (HPLC). Optimal conditions were 25ºC for 20 min with acetonitrile yielding maximum diazinon with 1/1mg/g MNP and dichloromethane 98.2%. Pesticide recovery with MNP was a low 54-64% (not acceptable), compared with 87% for HPLC.

 

Key words: diazinon residue, cibacron blue, modified magnetic nanoparticles, magnetic solid phase extractin, high performance liquid chromatography


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